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Showing 1 to 12 of 670 entries
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Sampling and extra-column effects in high-performance liquid chromatography; influence of peak skew on plate count calculations.

Journal of chromatographic science

Kirkland JJ, Yau WW, Stoklosa HJ, Dilks CH.
PMID: 893648
J Chromatogr Sci. 1977 Aug;15(8):303-16. doi: 10.1093/chromsci/15.8.303.

Chromatographic resolution and analysis accuracy can be seriously affected by broadening of very sharp bands associated with both high-performance size-exclusion chromatography and other liquid chromatography methods using less than 5 micron particles. The effect on column plate count by...

Simultaneous Quantification of 11 Constituents in Wuji Pill Using Ultra Performance Liquid Chromatography Coupled With a Triple Quadrupole Electrospray Tandem Mass Spectrometry.

Journal of chromatographic science

Tian T, Jin Y, Ma Y, Xie W, Xu H, Du Y.
PMID: 26363492
J Chromatogr Sci. 2016 Feb;54(2):237-45. doi: 10.1093/chromsci/bmv140. Epub 2015 Sep 12.

An ultra performance liquid chromatography coupled with a triple quadrupole electrospray tandem mass spectrometry (UPLC-MS-MS) method was developed for analyzing and identifying the constituents of 11 compounds including berberine, epiberberine, berberrubine, jatrorrhizine, coptisine, palmatine, evodiamine, rutaecarpine, limonin, paeoniflorin and...

An environmentally friendly method for the determination of pentachlorophenol in paper packaging materials using ultrasonic-assisted micellar extraction.

Journal of chromatographic science

Yang F, Li Z, Bian Z, Wang Y, Fan Z, Liu S, Zhang H, Tang G.
PMID: 26136274
J Chromatogr Sci. 2015 Nov-Dec;53(10):1808-12. doi: 10.1093/chromsci/bmv076. Epub 2015 Jun 30.

Ultrasonic-assisted micellar extraction coupled with high-pressure liquid chromatography has been developed for the determination of pentachlorophenol (PCP) in paper packaging materials. A non-ionic surfactant, polyethylene glycol sorbitan monolaurate (Tween 20), was used for ultrasonic extraction and the method was...

Improvement in Liquid Chromatographic Performance of Organic Polymer Monolithic Capillary Columns with Controlled Free-Radical Polymerization.

Journal of chromatographic science

Gama MR, Aggarwal P, Liu K, Lee ML, Bottoli CB.
PMID: 27993839
J Chromatogr Sci. 2017 Apr 01;55(4):398-404. doi: 10.1093/chromsci/bmw193.

Capillary columns containing butyl or lauryl methacrylate monoliths were prepared using two different free-radical polymerization methods: conventional free-radical polymerization and controlled/living free-radical polymerization, both initiated thermally, and these methods were compared for the first time. Both monolith morphology and...

Retention Characteristics of a pH Tunable Water Stationary Phase in Supercritical Fluid Chromatography.

Journal of chromatographic science

Scott AF, Thurbide KB.
PMID: 27993867
J Chromatogr Sci. 2017 Jan;55(1):82-89. doi: 10.1093/chromsci/bmw153. Epub 2016 Oct 07.

The retention characteristics of a novel pH tunable water stationary phase are presented. The method utilizes a change in mobile phase from N

Studies on Behaviors of Interactions Between New Polymer-based ZIC-HILIC Stationary Phases and Carboxylic Acids.

Journal of chromatographic science

Rasheed AS, Al-Phalahy BA, Seubert A.
PMID: 27993864
J Chromatogr Sci. 2017 Jan;55(1):52-59. doi: 10.1093/chromsci/bmw149. Epub 2016 Oct 07.

Zwitterionic stationary phases with nearly identical capacities were prepared by graft polymerization of a series of sulfobetaine precursors onto the surface of porous PS/DVB particles. The different spacer lengths are used as an investigative tool for the retention behavior...

Prepared polymethacrylate-based monoliths for the separation of cations by non-suppressed capillary ion chromatography.

Journal of chromatographic science

Li J, Zhu Y.
PMID: 23677716
J Chromatogr Sci. 2014 May-Jun;52(5):442-6. doi: 10.1093/chromsci/bmt056. Epub 2013 May 14.

This paper describes a novel analytical system for non-suppressed capillary ion chromatography. Methacrylate monolithic columns were prepared from silanized fused-silica capillaries of 320 µm i.d. by in situ polymerization of glycidyl methacrylate and ethylene dimethacrylate in the presence of...

Development and Validation of a New Stability-Indicating RP-UPLC Method for the Quantitative Determination of Bromfenac Sodium and Its Impurities in an Ophthalmic Dosage Form.

Journal of chromatographic science

Koppala S, Reddy VR, Anireddy JS.
PMID: 27270417
J Chromatogr Sci. 2016 Oct 17;54(9):1514-1521. doi: 10.1093/chromsci/bmw089.

A new rapid stability-indicating reversed-phase UPLC method was developed and validated for the determination of Bromfenac sodium and its impurities in Bromfenac ophthalmic solution. During literature search, only a few publications were found about Bromfenac sodium. There is no...

Effect of Chromatographic Conditions on Enantioseparation of Bedaquiline Using Polysaccharide-based Chiral Stationary Phases in RP-HPLC.

Journal of chromatographic science

Douša M, Reitmajer J, Lustig P, Štefko M.
PMID: 27071406
J Chromatogr Sci. 2016 Oct 17;54(9):1501-1507. doi: 10.1093/chromsci/bmw050.

A sensitive and specific high-performance liquid chromatography method for the separation and determination of bedaquiline stereoisomers has been developed and validated. Ten different chiral columns were tested in a reversed-phase system. Excellent enantioseparation with a resolution of all isomers...

Isolation, Chemical Fingerprinting and Simultaneous Quantification of Four Compounds from Tanacetum gracile Using a Validated HPLC-ESI-QTOF-Mass Spectrometry Method.

Journal of chromatographic science

Sharma N, Kumar C, Dutt P, Gupta S, Satti NK, Chandra S, Kitchlu S, Paul S, Vishwakarma RA, Verma MK.
PMID: 26951542
J Chromatogr Sci. 2016 May-Jun;54(5):796-804. doi: 10.1093/chromsci/bmw013. Epub 2016 Mar 06.

The present study was conducted to carry out the phytochemical investigation of Tanacetum gracile Hook. f. & Thomson and to develop a method for the simultaneous quantification of the isolated compounds in the extracts ofT. gracile growing in different...

A Validated HPTLC Densitometric Method for Simultaneous Determination of Evernic and Usnic Acids in Four Usnea Species and Comparison of Their Antioxidant Potential.

Journal of chromatographic science

Singh S, Khatoon S, Joshi Y, Prgyadeep S, Upreti DK, Rawat AKS.
PMID: 27418361
J Chromatogr Sci. 2016 Oct 17;54(9):1670-1677. doi: 10.1093/chromsci/bmw118.

A simple, sensitive and precise high-performance thin-layer chromatography method with densitometric detection was used for simultaneous determination of evernic (EV) and (+)-usnic acids (USN) in Usnea aciculifera (UA), U. ghattensis (UG), U. longissima (UL) and U. stigmatoides (US). This...

Rapid Fingerprint Analysis of Flos Carthami by Ultra-Performance Liquid Chromatography and Similarity Evaluation.

Journal of chromatographic science

Yu S, Zhu L, Xiao Z, Shen J, Li J, Lai H, Li J, Chen H, Zhao Z, Yi T.
PMID: 27377888
J Chromatogr Sci. 2016 Oct 17;54(9):1619-1624. doi: 10.1093/chromsci/bmw115.

Flos Carthami (FC), the dried flower of Carthamus tinctorius L., has widely been used for the treatment of cardiovascular diseases in China. A rapid fingerprint analysis method of FC was established by ultra-performance liquid chromatography (UPLC) for the quality...

Showing 1 to 12 of 670 entries